CaRIne Crystallography 3.1 Serial Key
CaRIne Crystallography 3.1 Serial Key
the crystal structure of moc was assigned by carine crystallography, directly from the diffraction data. the program uses the calculation function to simulate the reflections of the preliminary cells of the crystal structures. finally, the resulting cell parameters and atomic positions are refined. the initial structure of the crystal of was assigned, and the subsequent structure refinement was run using the following parameters: space group f m, pearson symbol
a large thin section (390 x 240 x 30μm) of the 96.4au-3ni-0.6ti interlayer/ysz interface between 0.5% si steel and 96.6ti interlayer was cut from the 100% ni steel. an approximately 1μm thick layer of the 96.6ti interlayer between the ysz layer and the steel was removed by using a diamond disk. the steel was oxidized in air and then cut into small pieces of less than 20x20x50μm. these small pieces were then surface-polished and etched in a solution of 30 vol% hcl. the depth of the 96.6ti interlayer was determined to be about 1μm by xrd and wds. the ratio of ni to ti in the 96.6ti interlayer was 80:20. phase identification was carried out by xrd and eds. the xrd peaks are shown in figure 3. the major phase of the 96.6ti interlayer was an au-rich alumina phase, denoted aual2o4. the formation of the 96.6ti interlayer consisted of solid solution of 98.9% au, 3.1% ni, and 0.2% ti in aual2o4, which was evidenced by the presence of ni and ti in the 96.6ti interlayer. the cr-si steel contained nanodomains of predominantly (100)-oriented anatase tio2 and cubic phase of sio2. the pt-cr-alloy interlayer contained a mixture of (100)-oriented phase of rutile tio2 and the (1011)-oriented one, as a phase of titanium nitride (tin). the phase compositions identified by eds are listed in table 1, which is summarized as follows.
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